참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Tert-Butylamine | HCID 6385 | — |
| 반응물 | 1-[4-(2-Chloroethoxy)phenyl]ethanone | HCID 13691191 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-[4-{-2-(1,1-Dimethylethylamino)-ethoxy}-phenyl]-ethanone | HCID 13691192 | — |
반응 단계
A mixture of 6.5 g of the product of Step A in 30 ml of tert.-butylamine was heated at 120° C. for 30 hours and was then diluted with water and extracted with ethyl acetate. The organic phase was washed with water, dried over a deshydrant, filtered and evaporated to dryness. The residue was chromatographed over silica and eluted with a 9-1 ethyl acetate-triethylamine mixture to obtain 7.264 g of 1-[4-{-2-(1,1-dimethylethylamino)-ethoxy}-phenyl]-ethanone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04853408 |
|---|
| 출처 데이터셋 | uspto-grants-1989_08 |
|---|
| ORD ID | ord-fca304eb29c24e84bbfaa78ddfa3439e |
|---|
| 출처 메모 | uspto-grants-1989_08 |
|---|
