Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → tert-Butyl (triphenylphosphoranylidene) acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | (tert-Butoxycarbonylmethyl)triphenylphosphonium Bromide | HCID 2733853 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | tert-Butyl (triphenylphosphoranylidene) acetate | HCID 256127 | 95.2% |
반응 단계
A suspension of the carbo-t-butoxymethyl triphenylphosphonium bromide (55.8 g, 122 mmol) in water (400 ml) was treated with sodium hydroxide (4.7 g, 117 mml) in water (100 ml). The mixture was stirred for 16 hours and the solid collected to give 43.7 g (95% of theory) of carbo-t-butoxymethylene triphenylphosphorane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04855086 |
| 출처 데이터셋 | uspto-grants-1989_08 |
| ORD ID | ord-ea072243946242229bc2a372745f0ad7 |
| 출처 메모 | uspto-grants-1989_08 |