1-Bromoisoquinoline → 1-Bromo-2-methylisoquinolinium tetrafluoroborate

HRID 1722583

반응식

HRID 1722583 반응식
[Br:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][N:3]=1.[F:12][B-:13]([F:16])([F:15])[F:14].[CH3:17][O+](C)C>C(Cl)Cl>[F:12][B-:13]([F:16])([F:15])[F:14].[Br:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][N+:3]=1[CH3:17]

참가 물질

4

반응물 2

HCID 6409631-BromoisoquinolineHCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)

생성물 1

HCID 200289711-Bromo-2-methylisoquinolinium tetrafluoroborate

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

The starting material was prepared by reaction of 1-bromoisoquinoline with trimethyloxonium tetrafluoroborate in CH2Cl2 to give 1-bromo-2-methylisoquinolinium tetrafluoroborate, m.p. 162°.

출처 및 근거

ORD 기록
ord-520341b9c73e4f978c28e0686a4c29d2
출처 데이터셋
uspto-grants-1989_08
특허 번호
US04855420

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