Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diketene → N-(2-morpholin-4-ylethyl)-3-oxobutanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diketene | HCID 12661 | — |
| 반응물 | 2-Morpholinoethylamine | HCID 408285 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | N-(2-morpholin-4-ylethyl)-3-oxobutanamide | HCID 4076516 | — |
반응 단계
To a solution of diketene (23.0 ml) in diethyl ether (115 ml) was added dropwise a solution of N-(2aminoethyl)morpholine (34.7 g) in diethyl ether (300 ml) at -40° C. After stirring for 2 hours at the same condition, the resulting precipitates were collected by filtration and dried in vacuo to give N-(2morpholinoethyl)acetoacetamide (41.1 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04857527 |
| 출처 데이터셋 | uspto-grants-1989_08 |
| ORD ID | ord-677f3f25c1d74e48aec7fe1e765794b7 |
| 출처 메모 | uspto-grants-1989_08 |