Hydrogen Peroxide → N-chloroacetamidomethyl acrylamide N,N-dimethyl acrylamide

HRID 1722991노트

반응식

HRID 1722991 반응식
[Cl:1][CH2:2][C:3]([NH:5][CH2:6][NH:7][C:8](=[O:11])[CH:9]=[CH2:10])=[O:4].[CH3:12][N:13]([CH3:18])[C:14](=[O:17])[CH:15]=[CH2:16].OO>CO>[Cl:1][CH2:2][C:3]([NH:5][CH2:6][NH:7][C:8](=[O:11])[CH:9]=[CH2:10])=[O:4].[CH3:12][N:13]([CH3:18])[C:14](=[O:17])[CH:15]=[CH2:16]

참가 물질

5

반응물 3

HCID 784Hydrogen PeroxideHCID 17587N,N-DimethylacrylamideHCID 86205169N-chloroacetamidomethyl acrylamide

생성물 1

HCID 86743307N-chloroacetamidomethyl acrylamide N,N-dimethyl acrylamide

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

21 g of N-chloroacetamidomethyl acrylamide, 14 g of N,N-dimethyl acrylamide, 850 g of methanol and 42 ml of a 33% hydrogen peroxide solution are placed in a Hanovia-type photochemical reactor equipped with a 100 W medium pressure lamp.

후처리

  1. customequipped with a 100 W medium pressure lamp

출처 및 근거

ORD 기록
ord-8eb33ae761e542dea811c1a498a16a70
출처 데이터셋
uspto-grants-1989_08
특허 번호
US04859460

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