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Triethylamine → N,N'-bis(allyl)carbodiimide

HRID 1723255
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반응식

HRID 1723255 반응식
[CH2:1]([NH:4][C:5]([NH:7][CH2:8][CH:9]=[CH2:10])=S)[CH:2]=[CH2:3].C(N(CC)CC)C.[I-].ClC1C=CC=C[N+]=1C>C(#N)C>[CH2:1]([N:4]=[C:5]=[N:7][CH2:8][CH:9]=[CH2:10])[CH:2]=[CH2:3]
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참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 1670692-Chloro-1-methylpyridinium iodideHCID 3034186Thiourea, N,N'-di-2-propen-1-yl-

생성물 1

HCID 13428060N,N'-bis(allyl)carbodiimide

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

1.56 g of N,N'-bis(allyl)thiourea, 2.4 g of triethylamine and 3.07 g of 2-chloro-1-methylpyridinium iodide are reacted in 40 ml of acetonitrile and the reaction mixture is worked up as described in Example 4. The product is obtained as a faintly yellowish oil.

후처리

  1. customThe product is obtained as a faintly yellowish oil

출처 및 근거

ORD 기록
ord-b1e719b11ff545e7ba7de4d2f9e2dd6e
출처 데이터셋
uspto-grants-1989_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04859761

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