Thionyl Chloride → HCID 20025664, 화합물

HRID 1723408노트

반응식

HRID 1723408 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]([OH:19])=O)=[CH:5][CH:4]=1.S(Cl)([Cl:22])=O>C(Cl)Cl>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]([Cl:22])=[O:19])=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 14555669HCID 14555669, 화합물

생성물 1

HCID 20025664HCID 20025664, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

To an ice-cold, stirring solution of 3 gm 9(4-methoxyphenyl)nonanoic acid in 10 ml. CH2Cl2 was added dropwise 1.2 ml thionyl chloride. The solution was then allowed to warm up to room temperature. The solvent and excess thionyl chloride were removed in vacuo to give a brown oil, which was used directly in the last step without further purification.

후처리

  1. customThe solvent and excess thionyl chloride were removed in vacuo
  2. customto give a brown oil, which
  3. customwas used directly in the last step without further purification

출처 및 근거

ORD 기록
ord-aab12e7043bc497c8d1a1db10757b098
출처 데이터셋
uspto-grants-1989_08
특허 번호
US04861798

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