참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 2,4,5-Trifluorobenzoyl chloride | HCID 145164 | — |
| 반응물 | Ethyl 3-(cyclopentylamino)buta-2-enoate | HCID 66962611 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | HCID 178472172 | HCID 178472172 | — |
반응 단계
Under ice cooling, triethylamine and 2,4,5-trifluorobenzoyl chloride were added to a solution of ethyl 3-(cyclopentylamino)buta-2-enoate in dioxane, for stirring at ambient temperature for 30 minutes and at 65° C. for one hour, to obtain ethyl 3-(cyclopentylamino)-2-(2,4,5-trifluorobenzoyl)buta-2-enoate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07488739B2 |
|---|
| 출처 데이터셋 | uspto-grants-2009_02 |
|---|
| ORD ID | ord-a74a10861c204c4ea7edab78d2610844 |
|---|
| 출처 메모 | uspto-grants-2009_02 |
|---|
