Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Diisopropylbenzene → 1,3-Diisopropylbenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Diisopropylbenzene | HCID 7450 | — |
| 반응물 | Mycophenolic acid glucuronide | HCID 6442661 | — |
| 반응물 | m-Diisopropylbenzene monohydroperoxide | HCID 71436539 | — |
| 생성물 | 1,3-Diisopropylbenzene | HCID 7450 | — |
| 생성물 | Hydroperoxide,1,1'-[1,3-phenylenebis(1-methylethylidene)]bis- | HCID 53471113 | — |
| 생성물 | m-Diisopropylbenzene monohydroperoxide | HCID 71436539 | — |
반응 단계
The raw material liquid for oxidation usually contains 20 to 60% by weight of m-diisopropylbenzene monohydroperoxide and 10 to 40% by weight of m-diisopropylbenzene. As usual reaction conditions, a temperature of 70 to 110° C., a pressure of 0 to 1 MPaG, a residence time of about 0.01 to 50 hours and the like are illustrated. As an apparatus used in the oxidation step, for example, a flowing type or batch type reaction vessel or reaction column can be listed. The oxidation reaction mixture obtained in the oxidation step usually contains 3 to 30% by weight of m-diisopropylbenzene dihydroperoxide and 20 to 60% by weight of m-diisopropylbenzene monohydroperoxide and 35% by weight or less of m-diisopropylbenzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07488853B2 |
| 출처 데이터셋 | uspto-grants-2009_02 |
| ORD ID | ord-84d300448354445b89e57a2f3dfe2257 |
| 출처 메모 | uspto-grants-2009_02 |