1,5-Dimethyltetralin → 1,5-Dimethylnaphthalene

HRID 1728996

반응식

HRID 1728996 반응식
[CH3:1][CH:2]1[C:11]2[C:6](=[C:7]([CH3:12])[CH:8]=[CH:9][CH:10]=2)[CH2:5][CH2:4][CH2:3]1.[H][H]>C1(C)C=CC=CC=1>[CH3:12][C:7]1[C:6]2[C:11](=[C:2]([CH3:1])[CH:3]=[CH:4][CH:5]=2)[CH:10]=[CH:9][CH:8]=1

참가 물질

4

반응물 2

HCID 895161,5-DimethyltetralinHCID 178418361HCID 178418361, 화합물

생성물 1

HCID 113061,5-Dimethylnaphthalene

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Using a 10% toluene solution of 1,5-dimethyltetralin obtained by the above method (A), dehydrogenation was conducted at 400° C. in a hydrogen atmosphere in the presence of a 0.3% Pt/Al2O3 catalyst for dehydrogenation to obtain 1,5-dimethylnaphthalene. Conversion of 1,5-dimethyltetralin was 100%, and selectivity to 1,5-dimethylnaphthalene was 97%.

후처리

  1. customobtained by the above method (A), dehydrogenation

출처 및 근거

ORD 기록
ord-09ed5b22c08648e59707d20750c9ac04
출처 데이터셋
uspto-grants-1994_07
특허 번호
US05329058

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