Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Phenylcyclohexane-1-carboxylic acid → Methyl 1-phenylcyclohexane-1-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Phenylcyclohexane-1-carboxylic acid | HCID 70817 | — |
| 반응물 | Methyl cyclopentanecarboxylate | HCID 78365 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Methyl 1-phenylcyclohexane-1-carboxylate | HCID 15105202 | — |
반응 단계
This compound was prepared (1.91 g, 8.76 mmol, 89%) from the product of Step A (2.00 g, 9.8 mmol) following the procedure for synthesis of methyl-1-cyclopentanecarboxylate as set forth in Step A, Example 1. The product of this step was homogeneous by TLC (ether:C2Cl2, 2:1) and used in the next step without further purification. CIMS 219 m/z (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05331010 |
| 출처 데이터셋 | uspto-grants-1994_07 |
| ORD ID | ord-a3d1cba68a344dc4abd002d70273a898 |
| 출처 메모 | uspto-grants-1994_07 |