Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
9,10-Anthracenedione, 1,2-dinitro- → 1-(p-Tert.-butyl-anilino)-6-nitro-anthraquinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 9,10-Anthracenedione, 1,2-dinitro- | HCID 42596 | — |
| 반응물 | 4-Tert-Butylaniline | HCID 69861 | — |
| 반응물 | 1,6-Dinitroanthraquinone | HCID 74146 | — |
| 용매 | 2-Methoxyethanol | HCID 8019 | — |
| 생성물 | 1-(p-Tert.-butyl-anilino)-6-nitro-anthraquinone | HCID 20316488 | — |
반응 단계
The product employed in a) can be obtained as follows: 15 g of 1,6-dinitro-anthraquinone and 30 ml of p-tert.-butylaniline are stirred at 125° C until no further dinitro-anthraquinone is detectable (approx. 6 hours being required). The warm mixture is diluted with 30 ml of ethylene glycol monomethyl ether, stirred until cold and filtered, and the residue is successively washed with ethylene glycol monomethyl ether and water. 13.9 g of 1-(p-tert.-butyl-anilino)-6-nitro-anthraquinone are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03989450 |
| 출처 데이터셋 | uspto-grants-1976_11 |
| ORD ID | ord-9de4435a2650493ea834b75ac03efc9b |
| 출처 메모 | uspto-grants-1976_11 |