Benzene → HCID 12906807, 화합물
반응식
[CH3:1][C:2]1([CH3:7])[NH:6][CH2:5][CH2:4][S:3]1.C1C=CC=CC=1.[Br:14][CH:15]([Br:19])[C:16](Cl)=[O:17].C(N(CC)CC)C>O>[CH3:1][C:2]1([CH3:7])[N:6]([C:16](=[O:17])[CH:15]([Br:19])[Br:14])[CH2:5][CH2:4][S:3]1참가 물질
6
실험 절차
To a mixture of 3.5 g. of 2,2-dimethyl thiazolidine, 50 ml. of benzene and 7.1 g. of dibromoacetyl chloride mixed in an ice bath was added 3.1 g. of triethylamine dropwise with stirring and continued cooling. When reaction was complete, the mixture was poured into water and the benzene layer separated, dried over magnesium sulfate and the benzene removed under vacuum. Yield was 8.5 g. of a dark oil.
후처리
- additionTo a mixture of 3.5 g
- additionwas added 3.1 g
- temperaturecontinued cooling
- customWhen reaction
- customthe benzene layer separated
- dry with materialdried over magnesium sulfate
- customthe benzene removed under vacuum
출처 및 근거
- ORD 기록
- ord-683d6c7f294c49fcb8b5e2468f1fc091
- 출처 데이터셋
- uspto-grants-1976_11
- 특허 번호
- US03989503
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