Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethylamine → 4-Ethylamino-3-nitrobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethylamine | HCID 6341 | — |
| 반응물 | 4-Chloro-3-nitrobenzamide | HCID 27942 | — |
| 생성물 | 4-Ethylamino-3-nitrobenzamide | HCID 3708922 | — |
반응 단계
II (160 g - 0.8 mole) was added portionwise with stirring at 60° C to 720 g of 50 % by weight aqueous ethylamine. The mixture was cooled, the precipitate was collected and crystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03989522 |
| 출처 데이터셋 | uspto-grants-1976_11 |
| ORD ID | ord-bb3097a7e15a44488e01fcb467723d81 |
| 출처 메모 | uspto-grants-1976_11 |