Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 3-(1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridin-2-yl)-N-phenylpropionic acid amide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | N-Phenylacrylamide | HCID 221792 | — |
| 반응물 | 1,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine | HCID 21498788 | — |
| 생성물 | 3-(1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridin-2-yl)-N-phenylpropionic acid amide | HCID 68139055 | — |
반응 단계
1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and N-phenyl acrylamide are reacted in accordance with the process described in Example 6. Reaction period 4 hours. M.P. of the hydrochloride of the title compound 207°-209° from 95% ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03991066 |
| 출처 데이터셋 | uspto-grants-1976_11 |
| ORD ID | ord-dfd3edd2b6e24ecda950bbbca3bb4bba |
| 출처 메모 | uspto-grants-1976_11 |