Phosphorus pentachloride → HCID 12329419, 화합물

HRID 1730105노트

반응식

HRID 1730105 반응식
[C:1]([C:4]1[CH:17]=[CH:16][CH:15]=[CH:14][C:5]=1[C:6]([O:8][O:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:7])(O)=[O:2].P(Cl)(Cl)(Cl)(Cl)[Cl:19]>C1C=CC=CC=1>[Cl:19][C:1]([C:4]1[CH:17]=[CH:16][CH:15]=[CH:14][C:5]=1[C:6]([O:8][O:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:7])=[O:2]

참가 물질

4

반응물 2

HCID 24819Phosphorus pentachlorideHCID 847692-[(Tert-butylperoxy)carbonyl]benzoic acid

생성물 1

HCID 12329419HCID 12329419, 화합물

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

To a suspension of t-butyl o-(carboxy)peroxybenzoate (16.2g. 0.06 moles) in 100 ml. of benzene at +6° to +24° C but preferably at +6° to +10° C was added in a single portion phosphorous pentachloride (12.6g. 0.06 moles).

출처 및 근거

ORD 기록
ord-84635f1a780f459496b1ad31ba408a1d
출처 데이터셋
uspto-grants-1976_11
특허 번호
US03991109

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