Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Bromodecane → Decyl thiocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Bromodecane | HCID 8173 | — |
| 반응물 | Sodium thiocyanate | HCID 516871 | — |
| 반응물 | Tricaprylylmethyl ammonium chloride | HCID 77620884 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Decyl thiocyanate | HCID 79301 | — |
반응 단계
A mixture of 100 grams (0.45 mole) of 1-bromodecane, 160 grams (1.98 moles)of sodium thiocyanate, 50 ml water and 10 grams of tricaprylylmethylammonium chloride was heated to 88°-105° C with stirring over a period of 2 hours. Examination of the reaction mixture by gas liquid partition chromatography showed that 100% conversionof the 1-bromodecane had occurred to give 1-thiocyanodecane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03992432 |
| 출처 데이터셋 | uspto-grants-1976_11 |
| ORD ID | ord-40daf765ff7f42f69c9e152c4d0c32ab |
| 출처 메모 | uspto-grants-1976_11 |