Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aminoacetaldehyde → 1-(alpha-Phenyl-o-tolyl)imidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aminoacetaldehyde | HCID 363 | — |
| 반응물 | Trimethyl orthoformate | HCID 9005 | — |
| 반응물 | 2-Benzylaniline | HCID 119805 | — |
| 촉매 | Titanium Tetrachloride | HCID 24193 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | 1-(alpha-Phenyl-o-tolyl)imidazole | HCID 21497358 | — |
반응 단계
In the manner given in Example 1, α-phenyl-o-toluidine is reacted first with trimethyl orthoformate; the resulting product is reacted with aminoacetaldehyde, dimethyl acetal, and the resulting product of this reaction is heated with titanium tetrachloride in monoglyme to give 1-(α-phenyl-o-tolyl)imidazole.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03992400 |
| 출처 데이터셋 | uspto-grants-1976_11 |
| ORD ID | ord-81a992cc110d4c3ca100eaea71f2ca7d |
| 출처 메모 | uspto-grants-1976_11 |