Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl orthoformate → 5-Methyl-1-[alpha-(o-chlorophenyl)-o-tolyl]imidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl orthoformate | HCID 31214 | — |
| 반응물 | (2-Methyl-1,3-dioxolan-2-yl)methanamine | HCID 12434663 | — |
| 반응물 | 2-[(2-Chlorophenyl)methyl]aniline | HCID 13426664 | — |
| 촉매 | Titanium Tetrachloride | HCID 24193 | — |
| 생성물 | 5-Methyl-1-[alpha-(o-chlorophenyl)-o-tolyl]imidazole | HCID 21497387 | — |
반응 단계
In the manner given in Example 3, α-(o-chlorophenyl)-o-toluidine is reacted with triethyl orthoformate, the resulting oil is heated with 2-methyl-2-(aminomethyl)-1,3-dioxolane, and the resulting product treated with titanium tetrachloride to give 5-methyl-1-[α-(o-chlorophenyl)-o-tolyl]imidazole.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03992400 |
| 출처 데이터셋 | uspto-grants-1976_11 |
| ORD ID | ord-cc13805fd1e8428d87430670069f7e86 |
| 출처 메모 | uspto-grants-1976_11 |