Hydrazine → HCID 178513179, 화합물

HRID 1730479노트

반응식

HRID 1730479 반응식
[ClH:1].Cl[C:3]1[CH:15]=[CH:14][C:6]([CH:7]=[N:8][NH:9][C:10](=[NH:13])SC)=[CH:5][CH:4]=1.[NH2:16][NH2:17]>C(O)C>[NH2:16][NH:17][C:10]([NH:9][NH:8][CH2:7][C:6]1[CH:14]=[CH:15][C:3]([Cl:1])=[CH:4][CH:5]=1)=[NH:13]

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 178504058HCID 178504058, 화합물

생성물 1

HCID 178513179HCID 178513179, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매2회

실험 절차

The same compound is synthesized by the reaction of equimolar quantities ofp-chlorobenzylhydrazine and methyl-3-(4-chlorobenzylidene)thiocarbazimidatehydrochloride (see Example 10) in hot ethanol. It is also prepared by the reaction of equimolar amounts of 1-(p-chlorobenzyl)-S-methylisothiosemicarbazide and hydrazine in warm ethanol, which affords 1-amino-3-(p-chlorobenzylamino)guanidine, followed by treatment of the latter with an equimolar quantity of p-chlorobenzaldehyde in hot isopropanol.

출처 및 근거

ORD 기록
ord-38468505759c4437af74da3fe5444d5c
출처 데이터셋
uspto-grants-1976_11
특허 번호
US03992446

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