N-Benzylideneaniline → HCID 53710483, 화합물

HRID 1730635노트

반응식

[C:1]1([CH3:20])[CH:6]=[CH:5][C:4]([C:7]2[O:11][C:10]3[C:12]4[C:17]([CH:18]=[CH:19][C:9]=3[CH:8]=2)=[CH:16][CH:15]=[CH:14][CH:13]=4)=[CH:3][CH:2]=1.[CH:21](=NC1C=CC=CC=1)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[C:1]1([CH:20]=[CH:21][C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH:2]=[CH:3][C:4]([C:7]2[O:11][C:10]3[C:12]4[C:17]([CH:18]=[CH:19][C:9]=3[CH:8]=2)=[CH:16][CH:15]=[CH:14][CH:13]=4)=[CH:5][CH:6]=1

참가 물질

반응물 2

HCID 10858N-Benzylideneaniline

HCID 203099572-(4-Methylphenyl)naphtho[1,2-b]furan

생성물 1

HCID 53710483HCID 53710483, 화합물

실험 절차

Following the procedure given in Example 1b the above-named 2-(p-tolyl)-naphtho-[1,2-b]furan was interacted with an equimolar quantity of benzalaniline to produce 2-(4-stilbenyl)naphtho[1,2-b]furan which, when crystallized from xylene and further purified by sublimation, melted at 228°-228.5° C. The wavelength of maximum excitation of this compound was 370 nm., and the wavelength of maximum emission was 426.

출처 및 근거

ORD 기록: ord-bfc09c56feaa49d28ade01b9ff372a24
출처 데이터셋: uspto-grants-1976_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03993645

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