2-Aminopyridine → HCID 20228667, 화합물

반응식

Br[CH2:2][C:3]([C:5]1[CH:6]=[CH:7][C:8]2[S:12][C:11](=[O:13])[N:10]([CH3:14])[C:9]=2[CH:15]=1)=O.[NH2:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][N:18]=1>>[N:16]1[C:3]([C:5]2[CH:6]=[CH:7][C:8]3[S:12][C:11](=[O:13])[N:10]([CH3:14])[C:9]=3[CH:15]=2)=[CH:2][N:18]2[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=12

참가 물질

반응물 2

HCID 104392-Aminopyridine

HCID 202286755-(Bromoacetyl)-3-methyl-1,3-benzothiazol-2(3H)-one

생성물 1

HCID 20228667HCID 20228667, 화합물수율 28.7%

실험 절차

5-(Imidazo[1,2-a]pyridin-2-yl)-3-methyl-2-benzothiazolinone (0.65 g) was prepared in the substantially same manner as that of Example 4 from 5-(2-bromoacetyl)-3-methyl-2-benzothiazolinone (2.3 g) and 2-aminopyridine (2.3 g).

출처 및 근거

ORD 기록: ord-d25b5e581fa74dbb8c110ad35b5fe870
출처 데이터셋: uspto-grants-1986_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04621084

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