Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1-(2-Amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | N-Boc-1-(2-amino-2-methylpropoxy)-2,2,5,5-tetramethyl cyclopentane | HCID 20165736 | — |
| 용매 | Trifluoroacetic acid | HCID 6422 | — |
| 생성물 | 1-(2-Amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane | HCID 20165755 | — |
반응 단계
N-Boc-1-(2-amino-2-methylpropoxy)-2,2,5,5-tetramethyl cyclopentane is dissolved in trifluoroacetic acid and stirred overnight. The solution is poured into 0 water and neutralized with 20% aqueous KOH. The mixture is extracted with ethyl acetate, dried over MgSO4, filtered and evaporated to give 1-(2-amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04622418 |
| 출처 데이터셋 | uspto-grants-1986_11 |
| ORD ID | ord-6b3416c251544d3a9a38682da2dae55b |
| 출처 메모 | uspto-grants-1986_11 |