3-Chloroaniline → Phenyl N-(3-chlorophenyl)carbamate
반응식
Cl[C:2]([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)=[O:3].[Cl:11][C:12]1[CH:13]=[C:14]([CH:16]=[CH:17][CH:18]=1)[NH2:15]>CCOCC>[Cl:11][C:12]1[CH:13]=[C:14]([NH:15][C:2](=[O:3])[O:4][C:5]2[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=2)[CH:16]=[CH:17][CH:18]=1참가 물질
4
실험 절차
A solution of 1.56 g of phenyl chloroformate in 50 ml of ether was added dropwise to a stirred solution of 2.55 g of 3-chloroaniline in 35 ml of ether. The mixture was stirred for one hour at room temperature and then filtered. The filtrate was evaporated and the residue crystallized from hexane to yield phenyl N-(3-chlorophenyl)-carbamate.
후처리
- filtrationfiltered
- customThe filtrate was evaporated
- customthe residue crystallized from hexane
출처 및 근거
- ORD 기록
- ord-189f4c9a6b34486988decc727ae8e42c
- 출처 데이터셋
- uspto-grants-1986_11
- 특허 번호
- US04623662
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