Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → N,N-Dimethylaminopropyl acrylamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | N-(3-dimethylaminopropyl)-3-methoxypropionamide | HCID 3097421 | — |
| 생성물 | N,N-Dimethylaminopropyl acrylamide | HCID 77452 | — |
반응 단계
188.3 g (1.0 mole) of N-(3-dimethylaminopropyl)-3-methoxypropionamide (according to Example 13 ) are heated with 1.5 g of sodium hydroxide at 90°-110° C. in a high vacuum. Within about 30 minutes methanol is split off, vigorous forming occurring. The temperature is increased and 103 g (0.66 mole=66% of the theoretical yield) of colorless oil having a Bp0.1 of 96°-100° C. are distilled off.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04237067 |
| 출처 데이터셋 | uspto-grants-1980_12 |
| ORD ID | ord-69b2edd453b647a8857b466efd7201f5 |
| 출처 메모 | uspto-grants-1980_12 |