HCID 13332658, 화합물 → 3-Hydroxymethyldibenzo[b,f]thiepin 5-oxide

반응식

[OH:1][CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:12]=[CH:11][C:10]3[CH:13]=[CH:14][CH:15]=[CH:16][C:9]=3[S:8][C:7]=2[CH:17]=1.[OH:18]CC1C=CC2CCC3C=CC=CC=3SC=2C=1>>[OH:1][CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:12]=[CH:11][C:10]3[CH:13]=[CH:14][CH:15]=[CH:16][C:9]=3[S:8](=[O:18])[C:7]=2[CH:17]=1

참가 물질

반응물 2

HCID 13332658HCID 13332658, 화합물

HCID 202555023-Hydroxymethyl-10,11-dihydrodibenzo[b,f]thiepin

생성물 1

HCID 133326573-Hydroxymethyldibenzo[b,f]thiepin 5-oxide

실험 절차

Repeat the process of Example 2, substituting an equivalent quantity of 3-hydroxymethyldibenzo[b,f]-thiepin for the 3-hydroxymethyl-10,11-dihydrodibenzo[b,f]thiepin, to obtain the title product (m.p., 146°-148° C.).

출처 및 근거

ORD 기록: ord-24804b3c036f4ad9b9a72da38e557d81
출처 데이터셋: uspto-grants-1980_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04237160

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