s-Triazolo(5,1-a)isoquinoline, 5,6-dihydro-2-phenyl- → s-Triazolo(5,1-a)isoquinoline, 2-phenyl-

HRID 1733135

반응식

HRID 1733135 반응식
[C:1]1([C:7]2[N:19]=[C:10]3[C:11]4[C:16]([CH2:17][CH2:18][N:9]3[N:8]=2)=[CH:15][CH:14]=[CH:13][CH:12]=4)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>C(OCC)(=O)C>[C:1]1([C:7]2[N:19]=[C:10]3[C:11]4[C:16]([CH:17]=[CH:18][N:9]3[N:8]=2)=[CH:15][CH:14]=[CH:13][CH:12]=4)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

3

반응물 1

HCID 134397s-Triazolo(5,1-a)isoquinoline, 5,6-dihydro-2-phenyl-

생성물 1

HCID 169678s-Triazolo(5,1-a)isoquinoline, 2-phenyl-수율 56%

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

Following substantially the same procedures of Example 58, and starting from 2-phenyl-5,6-dihydro-s-triazolo[5,1-a]isoquinoline, the title compound is prepared. Yield 56%, m.p. 157°-8° C. (from ethyl acetate).

출처 및 근거

ORD 기록
ord-e53c99a511c546e4a0d9d827663a7110
출처 데이터셋
uspto-grants-1980_12
특허 번호
USRE030456

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