참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Styrene | HCID 7501 | — |
| 반응물 | Dichloro(hexyl)silane | HCID 92038703 | — |
| 촉매 | HCID 178420539 | HCID 178420539 | — |
| 생성물 | n-Hexylphenethyldichlorosilane | HCID 20299100 | 91.1% |
반응 단계
3.80 g (20.5 millimol) of n-hexyldichlorosilane, 2.00 g (19.2 millimol) of styrene, and 0.023 g (1.92×10-5 mol) of tetrakis(triphenylphosphine)platinum (O) were introduced into a flask and reacted with stirring by heating in an oil bath at 60° C. for 8 hours and then subjected to distillation under a reduced pressure to produce 5.6 g (17.5 millimol) of n-hexylphenethyldichlorosilane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04242272 |
|---|
| 출처 데이터셋 | uspto-grants-1980_12 |
|---|
| ORD ID | ord-4683dd3e1a49444ebbe1ea160db91666 |
|---|
| 출처 메모 | uspto-grants-1980_12 |
|---|
