1,2,4-Oxadiazol-3-amine, 5-((2,6-dichlorophenyl)methyl)- → HCID 54050783, 화합물

HRID 1733479노트

반응식

HRID 1733479 반응식
[NH2:1][C:2]1[N:6]=[C:5]([CH2:7][C:8]2[C:13]([Cl:14])=[CH:12][CH:11]=[CH:10][C:9]=2[Cl:15])[O:4][N:3]=1.[CH:16]([O-])([O-])[O:17][CH2:18][CH3:19]>>[CH2:18]([O:17][CH:16]=[N:1][C:2]1[N:6]=[C:5]([CH2:7][C:8]2[C:13]([Cl:14])=[CH:12][CH:11]=[CH:10][C:9]=2[Cl:15])[O:4][N:3]=1)[CH3:19]

참가 물질

3

반응물 2

HCID 27431271,2,4-Oxadiazol-3-amine, 5-((2,6-dichlorophenyl)methyl)-HCID 53630039Ethylorthoformate2회

생성물 1

HCID 54050783HCID 54050783, 화합물

실험 절차

1 g of 3-amino-5-(2,6-dichlorobenzyl)-1,2,4-oxadiazole is heated in air at 150° C. for 3 hours with a few ml of ethyl orthoformate in an amount which is just sufficient to ensure slight agitation. The excess ethyl orthoformate is driven off under reduced pressure. The residue is crystallised from ether.

후처리

  1. customThe residue is crystallised from ether

출처 및 근거

ORD 기록
ord-614384af29274804a55aacaf18eba29c
출처 데이터셋
uspto-grants-1980_12
특허 번호
US04242352

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