Sulfuryl chloride → 4-methoxythiophene-3-carboxamide
반응식
[CH3:1][O:2][CH:3]1[C:7]([C:8]([NH2:10])=[O:9])=[CH:6][S:5][CH2:4]1.S(Cl)(Cl)(=O)=O>C(Cl)(Cl)(Cl)Cl>[CH3:1][O:2][C:3]1[C:7]([C:8]([NH2:10])=[O:9])=[CH:6][S:5][CH:4]=1참가 물질
4
실험 절차
1.59 parts of 3-methoxy-dihydrothiophene-4-carboxylic acid amide are reacted with 0.88 part by volume of sulfuryl chloride in 25 parts by volume of carbon tetrachloride in the course of 2 hours at 0° C. The end product is isolated from the reaction mixture by the method described in Example 1c. 1.17 parts (75% of theory) of 3-methoxythiophene-4-carboxylic acid amide are obtained.
후처리
- customThe end product is isolated from the reaction mixture by the method
출처 및 근거
- ORD 기록
- ord-4e37e738aa2643fdb6da8472a314929d
- 출처 데이터셋
- uspto-grants-1980_12
- 특허 번호
- US04242518
반응 노트
불러오는 중…