Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5-Dichloropentan-2-one → 3-Thiocyanato-5-chloro-2-pentanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5-Dichloropentan-2-one | HCID 94032 | — |
| 반응물 | Sodium thiocyanate | HCID 516871 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | 3-Thiocyanato-5-chloro-2-pentanone | HCID 10877693 | 96.3% |
반응 단계
A solution of 155.5 g (1 mole) of 3,5-dichloro-2-pentanone with 83 g (1.024 moles) of sodium rhodanide in 1 liter of methyl-ethyl-ketone is boiled for 1 hour under stirring. Then the procedure described in Example 1 is followed. 171 g (96.2%) of 3-thiocyanato-5-chloro-2-pentanone are obtained, which after distillation identical in all respect with the product of Example 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05534644 |
| 출처 데이터셋 | uspto-grants-1996_07 |
| ORD ID | ord-f9be7690b4644cacbc4da1e995704e76 |
| 출처 메모 | uspto-grants-1996_07 |