8-methyl-8H-thieno[2,3-b]indole-2-carboxylic acid → HCID 19068976, 화합물

HRID 1735091노트

반응식

HRID 1735091 반응식
[CH2:1]([N:8]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[C:10]2[CH:17]=[C:18]([C:20]([Cl:22])=[O:21])[S:19][C:9]1=2)C1C=CC=CC=1.CN1C2C(=CC=CC=2)C2C=C(C(O)=O)SC1=2>O=S(Cl)Cl>[CH3:1][N:8]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[C:10]2[CH:17]=[C:18]([C:20]([Cl:22])=[O:21])[S:19][C:9]1=2

참가 물질

4

반응물 2

HCID 20602328-methyl-8H-thieno[2,3-b]indole-2-carboxylic acidHCID 190689848-(Phenylmethyl)-8H-thieno[2,3-b]indole-2-carbonyl chloride

생성물 1

HCID 19068976HCID 19068976, 화합물

시약·촉매·용매 1

HCID 24386Thionyl Chloride용매

실험 절차

Preparation as described for (10) from (9) (2.0 g) and 20 ml SOCl2 gave 2.1 g (26) which was used without further purification.

후처리

  1. customPreparation

출처 및 근거

ORD 기록
ord-add87e693dbe43b293b29addcd1c68d0
출처 데이터셋
uspto-grants-1996_07
특허 번호
US05536721

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