Potassium Carbonate → HCID 849403, 화합물

HRID 1735100노트

반응식

[C:1]1([N:7]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[C:9]([CH:16]=O)=[C:8]2Cl)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C([O-])([O-])=O.[K+].[K+].[SH:25][CH2:26][C:27]([O:29][CH3:30])=[O:28]>>[C:1]1([N:7]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[C:9]3[CH:16]=[C:26]([C:27]([O:29][CH3:30])=[O:28])[S:25][C:8]2=3)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

반응물 3

HCID 11430Potassium Carbonate

HCID 16907Methyl Thioglycolate

HCID 3147932-chloro-1-phenyl-1H-indole-3-carbaldehyde

생성물 1

HCID 849403HCID 849403, 화합물수율 79.6%

실험 절차

Prepared from 1-Phenyl-2-chloroindole-3-carbaldehyde (0.90 g), K2CO3 (1.38 g) and methyl 2-mercaptoacetate (0.55 ml) yielding (51) 0.86 g (79.6%). M.p. 147°-149° C.

출처 및 근거

ORD 기록: ord-51c5797dfb814c7db10e6f6083df0931
출처 데이터셋: uspto-grants-1996_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05536721

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