1-(3-Chlorophenyl)ethanone → Benzenemethanol, 3-chloro-alpha,alpha-dimethyl-
반응식
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]([CH3:10])=[O:9])[CH:5]=[CH:6][CH:7]=1.[CH3:11][Mg]Br>O1CCCC1>[Cl:1][C:2]1[CH:3]=[C:4]([C:8]([OH:9])([CH3:11])[CH3:10])[CH:5]=[CH:6][CH:7]=1참가 물질
4
실험 절차
This compound is prepared in a manner analogous to that of Step A of this Example, using 13.9 grams (0.09 mole) of methyl 3-chlorophenyl ketone and 33.3 mL of methylmagnesium bromide (3.0M in diethyl ether) in 50 mL of dry tetrahydrofuran, yielding 2-(3-chlorophenyl)propan-2-ol.
후처리
- customThis compound is prepared in a manner analogous to that of Step A of this Example
출처 및 근거
- ORD 기록
- ord-1383baa454fd46bfa85dcdc1f298b355
- 출처 데이터셋
- uspto-grants-1996_07
- 특허 번호
- US05536725
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