Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5,6-Bis(phenylmethoxy)-1H-indole → 5,6-Dihydroxyindole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5,6-Bis(phenylmethoxy)-1H-indole | HCID 20920 | — |
| 반응물 | 5,6-Diacetoxyindole | HCID 3805883 | — |
| 촉매 | Iron | HCID 23925 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 5,6-Dihydroxyindole | HCID 114683 | — |
반응 단계
In a first stage, 5,6-diacetoxyindole and 5,6-dibenzyloxyindole are prepared by means of a cyclizing reduction. In the case of 5,6-dibenzyloxyindole the cyclizing reduction is carried out using iron in the presence of acetic acid. In a second stage, 5,6-dihydroxyindole is obtained:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05536865 |
| 출처 데이터셋 | uspto-grants-1996_07 |
| ORD ID | ord-df9f2491c8c54926a1cae643206f11a7 |
| 출처 메모 | uspto-grants-1996_07 |