Carbon Dioxide → HCID 54358079, 화합물

HRID 1735947노트

반응식

HRID 1735947 반응식
[CH2:1]([O:3][C:4](=[O:37])[C:5](=[NH:36])[CH:6](P(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1)[CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH3:2].[C:38](=O)=[O:39]>>[CH2:1]([O:3][C:4](=[O:37])[CH:5]([N:36]=[C:38]=[O:39])[CH2:6][CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:14])([CH3:15])[CH3:16])=[O:11])[CH3:2]

참가 물질

3

반응물 2

HCID 280Carbon DioxideHCID 178472716HCID 178472716, 화합물

생성물 1

HCID 54358079HCID 54358079, 화합물

반응 조건

온도
50 °C

실험 절차

The reaction solution from Example 9 is placed in a Parr® bomb and carbon dioxide (22 g, 0.5 mol) is condensed into the bomb. The bomb is sealed and heated to 50° C. for 12 hours. The bomb is cooled and vented to atmospheric pressure. The solution is transferred from the bomb to a flask and used as is in the next reaction (Example 11).

후처리

  1. customcondensed into the bomb
  2. customThe bomb is sealed
  3. temperatureThe bomb is cooled
  4. customThe solution is transferred from the bomb to a flask
  5. customas is in the next reaction (Example 11)

출처 및 근거

ORD 기록
ord-faeadfd5a0604f41986fed3e3c12fa5d
출처 데이터셋
uspto-grants-1996_07
특허 번호
US05539082

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