Sodium azide ammonium chloride → HCID 178441507, 화합물

HRID 1736887노트

반응식

HRID 1736887 반응식
[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][C:20]([Cl:23])=[CH:19][C:18]=3[C:24]#[N:25])=[CH:13][CH:12]=2)[C:8]2[CH:26]=[C:27]([N:30]([CH3:40])[C:31]([NH:33][CH:34]3[CH2:39][CH2:38][CH2:37][CH2:36][CH2:35]3)=[O:32])[CH:28]=[CH:29][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4].[Cl-].[NH4+].[N-:43]=[N+:44]=[N-:45].[Na+]>>[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][C:20]([Cl:23])=[CH:19][C:18]=3[C:24]3[NH:45][N:44]=[N:43][N:25]=3)=[CH:13][CH:12]=2)[C:8]2[CH:26]=[C:27]([N:30]([CH3:40])[C:31]([NH:33][CH:34]3[CH2:35][CH2:36][CH2:37][CH2:38][CH2:39]3)=[O:32])[CH:28]=[CH:29][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4]

참가 물질

3

반응물 2

HCID 21923157Sodium azide ammonium chlorideHCID 572513924'-[(2-n-butyl-6-(N-cyclohexylaminocarbonyl-methyl-amino)-benzimidazol-1-yl)-methyl]-4-chloro-2-cyano-biphenyl

생성물 1

HCID 178441507HCID 178441507, 화합물

실험 절차

Prepared in analogous manner to Example 59 from 4'-[(2-n-butyl-6-(N-cyclohexylaminocarbonyl-methyl-amino)-benzimidazol-1-yl)-methyl]-4-chloro-2-cyano-biphenyl and ammonium chloride/sodium azide.

출처 및 근거

ORD 기록
ord-7a8391fecb304ee4a854ac84f554f835
출처 데이터셋
uspto-grants-1996_07
특허 번호
US05541229

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