참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-(1-Dodecen-1-yl)dihydro-2,5-furandione | HCID 32933 | — |
| 반응물 | 3-Amino-1,2-propanediol | HCID 73561 | — |
| 촉매 | Sodium Methoxide | HCID 10942334 | — |
| 생성물 | Dodecenyl 3-imino-1,2-propanediol succinate | HCID 86749673 | 172.6% |
반응 단계
A 100 ml four necked round bottom flask equipped with a mechanical stirrer, thermometer, nitrogen inlet and short path distillation head was charged with 3-amino-l,2-propandiol (8.0 g, 8.78×10-2 mole), dodecenyl succinic anhydride (23.4 g, 8.78×10-2 mole) and sodium methoxide (0.05 g, 9.26×10-4 mole). The reaction mixture was heated to 135° C. for 6 hours under a mild nitrogen blanket giving 28.3 g (94.9% yield) of dodecenyl 3-imino-1,2-propanediol succinate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US05541341 |
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| 출처 데이터셋 | uspto-grants-1996_07 |
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| ORD ID | ord-4b00def0ea71418997f8c3de78e13c89 |
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| 출처 메모 | uspto-grants-1996_07 |
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