2-Naphthalenesulfonyl chloride → Methyl 4-[(2-naphthylsulfonyl)amino]butanoate

HRID 1738856노트

반응식

HRID 1738856 반응식
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[S:11](Cl)(=[O:13])=[O:12].[NH2:15][CH2:16][CH2:17][CH2:18][C:19]([O:21][CH3:22])=[O:20]>>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[S:11]([NH:15][CH2:16][CH2:17][CH2:18][C:19]([O:21][CH3:22])=[O:20])(=[O:13])=[O:12]

참가 물질

3

반응물 2

HCID 71252-Naphthalenesulfonyl chlorideHCID 18614Methyl 4-aminobutanoate

생성물 1

HCID 4204457Methyl 4-[(2-naphthylsulfonyl)amino]butanoate수율 94%

실험 절차

Using an analogous procedure to that described in Example 2, 2-naphthylsulphonyl chloride was reacted with methyl 4-aminobutyrate to give methyl 4-(2-naphthalenesulphonamido)butyrate in 94% yield.

출처 및 근거

ORD 기록
ord-85312ef953dd41938ab49ed251f0e2d7
출처 데이터셋
uspto-grants-1999_10
특허 번호
US05965559

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