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Tert-Butylamine → HCID 54713534, 화합물

HRID 1740715
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HRID 1740715 반응식
[OH:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[NH:5][C:4](=[O:12])[C:3]=1[C:13]([O:15]C)=O.[C:17]([NH2:21])([CH3:20])([CH3:19])[CH3:18]>C(O)C>[C:17]([NH:21][C:13]([C:3]1[C:4](=[O:12])[NH:5][C:6]2[C:11]([C:2]=1[OH:1])=[CH:10][CH:9]=[CH:8][CH:7]=2)=[O:15])([CH3:20])([CH3:19])[CH3:18]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 6385Tert-ButylamineHCID 54676766Methyl 4-hydroxy-2-oxo-1,2-dihydroquinoline-3-carboxylate

생성물 1

HCID 54713534HCID 54713534, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

8.76 g (0.04 mol) of methyl 4-hydroxy-2-oxoquinoline-3-carboxylate was stirred with 3.7 g (0.05 mol) of tert-butylamine in 60 ml of ethanol in a miniautoclave for 8 hours at 150° C. under autogenous pressure. After cooling, the crystals were removed by suction filtration, washed with ligroin and dried.

후처리

  1. temperatureAfter cooling
  2. customthe crystals were removed by suction filtration
  3. washwashed with ligroin
  4. customdried

출처 및 근거

ORD 기록
ord-fd9c455cfe9942979d5f98b368148a6a
출처 데이터셋
uspto-grants-1999_10
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05972841

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