Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine → Methyl 6-amino-4-chloropyridine-2-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine | HCID 9321 | — |
| 반응물 | 2,6-Dimethyl 4-chloropyridine-2,6-dicarboxylate | HCID 237845 | — |
| 생성물 | Methyl 6-amino-4-chloropyridine-2-carboxylate | HCID 9899037 | — |
반응 단계
4-Chloropyridine-2,6-dicarboxylic acid, dimethyl ester (230 mg, 1 mmol) was converted to the monoacyl hydrazide by adding one-half equivalent of anyhydrous hydrazine. The monohydrazide was converted to the monoacyl azide by the methodology described in step B of Example 35. The title compound was obtained by applying the methodology described in step C of Example 35.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05972975 |
| 출처 데이터셋 | uspto-grants-1999_10 |
| ORD ID | ord-2efef7372d9341a2ae44ac5686064290 |
| 출처 메모 | uspto-grants-1999_10 |