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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1742775생성일: 2026년 10월 26일

Epichlorohydrin → 2-[(4-Benzoylphenoxy)methyl]oxirane

https://huagongshe.com/reaction/1742775

반응식

참여 물질

역할이름HCID투입량
반응물EpichlorohydrinHCID 7835—
반응물4-HydroxybenzophenoneHCID 14347—
반응물Sodium HydroxideHCID 14798—
생성물2-[(4-Benzoylphenoxy)methyl]oxiraneHCID 35281683%

반응 조건

온도100 °C

반응 단계

1 g of 4-hydroxy benzophenone and 4.668 g of epichlorohydrin (0.025 mol) were dissolved, 20.5 mg of sodium hydroxide was added, and the reaction system was heated to 100° C. and then cooled to 95° C. Furthermore 201.4 mg of sodium hydroxide was added, and additional heating and agitation was carried out for 3 hours. The system was cooled to the room temperature, and salt was removed by filtering. The obtained filtrate was condensed under reduced pressure condition, and purified according to the silica gel chromatography to obtain 1.0 g of solid state 4-glycidyloxy benzophenone (Yield: 83%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05342610
출처 데이터셋uspto-grants-1994_08
ORD IDord-e85f38e65d7646519f71c006d78eed22
출처 메모uspto-grants-1994_08