Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isopropyl iodide → 2-Nitro-5-(2-propyloxy)benzyl alcohol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isopropyl iodide | HCID 6362 | — |
| 반응물 | 3-(Hydroxymethyl)-4-nitrophenol | HCID 108946 | — |
| 생성물 | 2-Nitro-5-(2-propyloxy)benzyl alcohol | HCID 54487340 | — |
반응 단계
10 g (60 mmol) of 5-hydroxy-2-nitrobenzyl alcohol were reacted with 7.0 ml (70 mmol) of isopropyl iodide analogously to Example 4a); after purification over silica gel with n-heptane/ethyl acetate (3:2), 10.3 g of oily crude product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05726305 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-61857a4aa4ad49af8aac9e9223a18f71 |
| 출처 메모 | uspto-grants-1998_03 |