HCID 71230594, 화합물 → HCID 71230585, 화합물
반응식
[O:1]=[C:2]1[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][NH:11][C:12](=[O:18])[O:13][C:14]([CH3:17])([CH3:16])[CH3:15])[C:5](=[O:19])[NH:4][NH:3]1>C(Cl)Cl>[O:1]=[C:2]1[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][NH:11][C:12](=[O:18])[O:13][C:14]([CH3:15])([CH3:16])[CH3:17])[C:5](=[O:19])[N:4]=[N:3]1참가 물질
3
실험 절차
To tert-butyl 4-(3,5-dioxo-1,2,4-triazolidin-4-yl)butylcarbamate (15 mg, 0.055 mmol) in CH2Cl2 (0.551 mL) was added SiO2—HNO3 (35 mg). The mixture was stirred at room temperature for 15 minutes, then filtered, concentrated in vacuo and dried, giving tert-butyl 4-(3,5-dioxo-3H-1,2,4-triazol-4(5H)-yl)butylcarbamate (I-8c: 15 mg, quantitative yield) as a red oil.
후처리
- filtrationfiltered
- concentrationconcentrated in vacuo
- customdried
출처 및 근거
- ORD 기록
- ord-34bbf236d8dd44e88527afdd3f1e4d10
- 출처 데이터셋
- uspto-grants-2015_10
- 특허 번호
- US09149541B2
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