2-Amino-1,2-diphenylethanol → HCID 58080370, 화합물
반응식
[N:1]1([C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH2:6][CH2:5][CH:4]([C:7]([O-:9])=O)[CH2:3][CH2:2]1.[NH2:17][CH:18]([C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)[CH:19]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)O>>[C:27]1([C:18]2[N:17]=[C:7]([CH:4]3[CH2:3][CH2:2][N:1]([C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH2:6][CH2:5]3)[O:9][C:19]=2[C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=2)[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=1참가 물질
3
실험 절차
Starting from 1.08 g of mono-tert-butyl piperidine-1,4-dicarboxylate and 1 g 2-amino-1,2-diphenyl-ethanol the product may be prepared as described in the literature (cf. Tet. 2001, 4867). The product is purified by chromatography (method B). 560 mg are obtained in the form of an oil. Analytical HPLC-MS (method A): RT=1.72 min.
후처리
- custommay be prepared
- customThe product is purified by chromatography (method B)
- custom560 mg are obtained in the form of an oil
출처 및 근거
- ORD 기록
- ord-4d5a96054dfc41b4ab538d5659f3bea7