6-chloro-2-N,4-N-dipropyl-1,3,5-triazine-2,4-diamine → HCID 57377914, 화합물

HRID 1752135노트

반응식

HRID 1752135 반응식
Cl[C:2]1[N:7]=[C:6]([NH:8][CH2:9][CH2:10][CH3:11])[N:5]=[C:4]([NH:12][CH2:13][CH2:14][CH3:15])[N:3]=1.Cl.[CH2:17]([O:21][NH:22][CH3:23])[CH:18]([CH3:20])[CH3:19]>>[CH2:13]([NH:12][C:4]1[N:5]=[C:6]([NH:8][CH2:9][CH2:10][CH3:11])[N:7]=[C:2]([N:22]([CH3:23])[O:21][CH2:17][CH:18]([CH3:20])[CH3:19])[N:3]=1)[CH2:14][CH3:15]

참가 물질

3

반응물 2

HCID 183046-chloro-2-N,4-N-dipropyl-1,3,5-triazine-2,4-diamineHCID 86665985HCID 86665985, 화합물

생성물 1

HCID 57377914HCID 57377914, 화합물수율 82%

실험 절차

2-Chloro-N-(4,6-bis-(n-propylamino)-[1,3,5]triazine (XXXIV) was reacted with O-isobutyl-N-methyl-hydroxylamine hydrochloride as described in Example 13, affording LXXXII in 82% yield. ESI-MS (m/z) 297 [M+H]+.

후처리

  1. customaffording LXXXII in 82% yield

출처 및 근거

ORD 기록
ord-206704d3bcab4541953bcdf1f63a6761
출처 데이터셋
uspto-grants-2015_10
특허 번호
US09162992B2

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