Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Nitrotoluene → Azoxybenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Nitrotoluene | HCID 6944 | — |
| 반응물 | Nitrobenzene | HCID 7416 | — |
| 반응물 | 1-Ethyl-2-nitrobenzene | HCID 69156 | — |
| 생성물 | Azoxybenzene | HCID 10316 | — |
반응 단계
The reduction reaction was carried out in the same manner as set forth in Example 6 except for using a mixture of 1.0 mmol of o-methyl nitrobenzene and 1.0 mmol of o-ethyl nitrobenzene instead of using nitrobenzene alone, and using 19.5 mg (the amount required for swelling of the reactant in 100%) of Polymer supported reagent-2, and thereby an azoxybenzene derivative of a symmetrical structure and an azoxybenzene derivative of an asymmetrical structure were obtained as a main product, respectively.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09169200B2 |
| 출처 데이터셋 | uspto-grants-2015_10 |
| ORD ID | ord-5640dc0bf2034804ae5f5c51180f0889 |
| 출처 메모 | uspto-grants-2015_10 |