HCID 15341803, 화합물 → HCID 15341818, 화합물

HRID 1756207노트

반응식

HRID 1756207 반응식
[OH:1][C:2]1[C:10]([CH2:11][CH:12]=[CH2:13])=[C:9]([OH:14])[CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5]>[Pd].C(O)C>[OH:1][C:2]1[C:10]([CH2:11][CH2:12][CH3:13])=[C:9]([OH:14])[CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5]

참가 물질

4

반응물 1

HCID 15341803HCID 15341803, 화합물

생성물 1

HCID 15341818HCID 15341818, 화합물수율 74%

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

2,4-Dihydroxy-3-(2-propenyl)benzamide (575 mg) and 125 ml of ethanol was hydrogenated at 5 psi, room temperature, using 4% Pd/C catalyst for 3 hours. The solvent was removed under vacuum to give the product as an oil (4.25 mg, 74%).

후처리

  1. customwas hydrogenated at 5 psi, room temperature
  2. customfor 3 hours
  3. customThe solvent was removed under vacuum

출처 및 근거

ORD 기록
ord-813866da66e14739b829e39805f2dc8e
출처 데이터셋
uspto-grants-1995_08
특허 번호
US05439937

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