Ethyl acetate hexane → HCID 22399579, 화합물

HRID 1756226노트

반응식

HRID 1756226 반응식
[NH2:1][C:2]([C:4]1[CH:31]=[CH:30][C:7]([O:8][CH2:9][CH2:10][CH2:11][O:12][C:13]2[CH:26]=[CH:25][C:16]3[CH:17]=[CH:18][CH:19]([C:21]([O:23][CH3:24])=[O:22])[O:20][C:15]=3[C:14]=2[CH2:27][CH2:28][CH3:29])=[C:6]([CH2:32][CH:33]2[CH2:35][CH2:34]2)[C:5]=1[OH:36])=[O:3].[C:37](OCC)(=O)C.CCCCCC>>[NH2:1][C:2]([C:4]1[CH:31]=[CH:30][C:7]([O:8][CH2:9][CH2:10][CH2:11][O:12][C:13]2[CH:26]=[CH:25][C:16]3[CH:17]=[CH:18][CH:19]([C:21]([O:23][CH3:24])=[O:22])[O:20][C:15]=3[C:14]=2[CH2:27][CH2:28][CH3:29])=[C:6]([CH2:32][CH:33]2[CH2:35][CH2:34]2)[C:5]=1[O:36][CH3:37])=[O:3]

참가 물질

3

반응물 2

HCID 21226206Ethyl acetate hexaneHCID 22399592HCID 22399592, 화합물

생성물 1

HCID 22399579HCID 22399579, 화합물

실험 절차

The compound of Example 67 is exposed to the conditions described in Example 25. Chromatography of the crude product on silica gel using ethyl acetate/hexane, (3:7) as eluant affords the product.

후처리

  1. customaffords the product

출처 및 근거

ORD 기록
ord-749f14c520d240d9b49162ed08aec698
출처 데이터셋
uspto-grants-1995_08
특허 번호
US05439937

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