Thionyl Chloride → HCID 54108381, 화합물
반응식
[CH:1]([C:4]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]([CH3:14])[CH3:13])[C:5]=1[CH2:6]O)([CH3:3])[CH3:2].S(Cl)([Cl:17])=O>C1(C)C=CC=CC=1>[CH:1]([C:4]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]([CH3:14])[CH3:13])[C:5]=1[CH2:6][Cl:17])([CH3:3])[CH3:2]참가 물질
4
실험 절차
To a solution of 1.37 g (7.12 mmol) of 2, 6-diisopropylbenzyl alcohol in 20 ml of toluene was added 0.78 ml (10.7 mmol) of thionyl chloride, and the resultant mixture was stirred at room temperature for 3.5 hours. The reaction mixture was washed with water, dried over anhydrous magnesium sulfate and the solvent evaporated in vacuo to give 1.49 g of 2, 6-diisopropylbenzyl chloride as an oil.
후처리
- washThe reaction mixture was washed with water
- dry with materialdried over anhydrous magnesium sulfate
- customthe solvent evaporated in vacuo
출처 및 근거
- ORD 기록
- ord-23c7f3a620a7481f9b504a21409aa50a
- 출처 데이터셋
- uspto-grants-1995_08
- 특허 번호
- US05442060
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